Title:Advanced Organic Synthesis. Methods and Techniques by R.S. Monson (Repost)
Author:Advanced Organic Synthesis, R.S. Monson
Pages: Pages: 313
Description:The purpose of this text is to provide a survey, and systematic introduction to, the modern techniques of organic synthesis for the advanced undergraduate student or the beginning graduate student. An attempt has been made to acquaint the student with a variety of laboratory techniques as well as to introduce him to chemical reagents that require deftness and care in handling.
Experiments have been drawn from the standard literature of organic synthesis including suitable modifications of several of the reliable and useful preparations that have appeared in “Organic Synthesis,” Other examples have been drawn from the original literature. Where ever possible, the experiments have been adapted to the locker complement commonly found in the advanced synthesis course employing intermediate scale standard taper glassware. Special equipment for the performance of some of the syntheses would include low-pressure hydrogenation apparatus, ultraviolet lamps and reaction vessels. Dry Ice (cold finger) condensers, vacuum sublimation and distillation apparatus, and spectroscopic and chromato- graphic instruments. In general, an attempt has been made to employ as substrates materials that are available commercially at reasonable cost, although several of the experiments require precursor materials whose preparation is detailed in the text. Some of the reagents are hazardous to handle, but I believe that, under reasonable supervision, advanced students will be able to perform the experiments with safety.
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